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In this episode, Mike is joined by Support Chemist Ashley Jones and Stock Production Manager Thomas Kozikowski to tackle listener-submitted questions from the lab. First, they unpack whether a standard additions curve from one sample can be applied to others—exploring when it’s valid, what risks come with instrument drift, and why true matrix matching matters. Then, they take on a tough scenario: how to handle high-throughput analysis of true unknown mineral samples using ICP-OES and ICP-MS. From digestion techniques and fusion methods to internal standard selection, interference management, and data review strategies, the team offers practical solutions for demanding analytical workflows.

If you’ve ever faced the challenge of balancing accuracy with efficiency in the lab, this episode is a must-listen.

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In this episode, we tackle real-world technical support questions submitted by listeners. Joined by R&D Chemists Liv Forbes & Autumn Phillips and Tech Support Chemist Ashley Jones, we explore three unique challenges:

• Stabilizing nitrite (NO₂) standards for ion chromatography and why pH control is the key to preventing unwanted oxidation.
• Calculating tolerance intervals, including how to use statistical tools to set confident, population-based limits in your data.
• Troubleshooting tungsten recovery in high-molybdenum matrices on ICP-OES, covering the role of internal standards, acid chemistry, and smarter wavelength selection.

From practical lab prep tips to advanced troubleshooting insights, this episode is packed with knowledge you can put into action right away.

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In this episode of our Back to Basics series, we explore the critical role of tuning solutions, check solutions, and calibration standards in ICP-OES and ICP-MS. Joined by R&D Chemists Liv Forbes & Autumn Phillips and Tech Support Chemist Ashley Jones, we break down why proper calibration and routine checks are essential to maintaining instrument performance and ensuring accurate, reliable data. From wavelength and mass calibration to tuning for sensitivity and minimizing interferences, to building stable, well-matched calibration standards—this conversation covers the practices that keep your results trustworthy.

Whether you’re fine-tuning methods or setting up your lab for long-term success, this episode delivers the knowledge you need to keep your instruments performing at their best.

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